Process for the manufacture of dicalcium phosphate Download PDF Info ... phosphoric acid slurry dicalcium phosphate weight Prior art date 1957-01-28 Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Read MoreThe invention relates to a combined process for the manufacture of feed grade dicalcium phosphate and pure phosphoric acid. The process comprises the reaction of an excess of phosphate rock with aqueous solutions of a mineral acid selected from hydrochloric acid, phosphoric acid and nitric acid, characterized by the fact that the free acidity of the dissolution liquor does not exceed 60% and ...
Read MoreThe invention relates to a combined process for the manufacture of feed grade dicalcium phosphate and pure phosphoric acid. The process comprises the reaction of an excess of phosphate rock with aqueous solutions of a mineral acid selected from hydrochloric acid, phosphoric acid and nitric acid, characterized by the fact that the free acidity of the dissolution liquor does not exceed 60% and ...
Read MoreUS4141958A US05/836,370 US83637077A US4141958A US 4141958 A US4141958 A US 4141958A US 83637077 A US83637077 A US 83637077A US 4141958 A US4141958 A US 4141958A Authority US United States Prior art keywords phosphoric acid phosphate organic solvent sub monocalcium phosphate Prior art date 1976-02-06 Legal status (The legal status is an assumption and is not a
Read Morecalcium phosphate phosphate phosphoric acid calcium mono Prior art date 1934-07-02 Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.) Expired - Lifetime Application number US733475A Inventor Harry A Curtis
Read MoreUS1235025A US9460216A US9460216A US1235025A US 1235025 A US1235025 A US 1235025A US 9460216 A US9460216 A US 9460216A US 9460216 A US9460216 A US 9460216A US 1235025 A US1235025 A US 1235025A Authority US United States Prior art keywords calcium phosphate making dicalcium phosphate mixture Prior art date 1916-05-01 Legal status (The legal status is an
Read MoreThis patent also discloses a process wherein naturally occurring phosphate is reacted with phosphoric acid and the product is treated with acetic or oxalic acid. DISCLOSURE OF THE INVENTION: 0) Dicalcium phosphate substantially free of fluorides is prepared by a novel process which particularly avoids production of unwanted calcium chloride as ...
Read MoreDicalcium phosphate shows the most commonly used production method is known as the “wet acid” route in which rock phosphate is reacted with sulphuric acid to produce phosphoric acid. After concentration and purification to reduce the level of undesirable elements, this phosphoric acid is
Read MoreFollow this APPLICATION TO DICALCIUM PHOSPHATE PROCESS. 43 The manufacturing coats for the normal superphosphate plant are taken from Rounsley (43). dicalcium phosphate production line . Aug 2, 2016 Phosphoric acid is the intermediary product for the manufacturing process of dicalcium phosphate machinery Dicalcium Phosphate, World News .
Read MoreDicalcium phosphate shows the most commonly used production method is known as the “wet acid” route in which rock phosphate is reacted with sulphuric acid to produce phosphoric acid. After concentration and purification to reduce the level of undesirable elements, this phosphoric acid is
Read MoreFollow this APPLICATION TO DICALCIUM PHOSPHATE PROCESS. 43 The manufacturing coats for the normal superphosphate plant are taken from Rounsley (43). dicalcium phosphate production line . Aug 2, 2016 Phosphoric acid is the intermediary product for the manufacturing process of dicalcium phosphate machinery Dicalcium Phosphate, World News .
Read MoreA method of producing dicalcium phosphate from calcium phosphate includes reacting the calcium phosphate with a mineral acid such as sulphuric acid to produce a calcium salt and phosphoric acid. The calcium salt may then be hydrolyzed to form a calcium alkali which may then be reacted with the phosphoric acid to produce dicalcium phosphate.
Read MoreThis patent also discloses a process wherein naturally occurring phosphate is reacted with phosphoric acid and the product is treated with acetic or oxalic acid. DISCLOSURE OF THE INVENTION: 0) Dicalcium phosphate substantially free of fluorides is prepared by a novel process which particularly avoids production of unwanted calcium chloride as ...
Read Morephosphoric acid and depositing it on a slow moving covered conveyor belt (den). The production was 165,000 mtpy. • The share of dicalcium phosphate precipitated from bones and used as animal feed, is estimated in the order of 10-15% of the total amount of 720.000- 750.000 tons in Western Europe. Process Functions • Dicalcium phosphate ...
Read MoreThis invention relates to an improved process for the recovery of dicalcium phosphate from phosphate rock or ore. Various wet processes for producing phosphoric acid by acid treating phosphate rock have been described in the literature, such as in Phosphoric Acid edited by A. B. Slack (Marcel Dekker, Inc., New York, 1968).
Read MoreA new process to produce defluorinated dicalcium phosphate (DCP) using phosphate rock concentrate has been developed. This new process has as main characteristic the low concentration of P 2 O 5 in the liquid phase. The process comprises three main steps: solubilization of the phosphate rock concentrate with sulfuric acid, defluorination of the phosphoric acid solution with potassium
Read MoreAn investigation was undertaken to develop a process for producing di-calcium phosphate by direct acidulation of phosphate rock. In general, when phosphate rock is treated with sulfuric acid, mono-calcium phosphate or phosphoric acid is formed. If less sulfuric acid is used, di-calcium phosphate should be formed
Read MoreApr 01, 1994 The clear solution containing mainly a weak phosphoric acid is then neutralized, in the third step, in order to produce the final dicalcium phosphate product. After filtration the dicalcium phosphate is dried and the mother licquor is recycled to the first step of the process, the phosphate
Read MoreFlow diagram of Dihydrate Process (EFMA, 2000a)-Hydrochloric Acid Route: Phosphoric acid can also be produced by digestion of beneficiated phosphate rock with hydrochloric acid as in following ...
Read MoreWet process phosphoric acid is produced from reaction of sulphuric acid and rock phosphate. It can be used for the manufacture of feed grade monodicalcium phosphate (MDCP) / dicalcium phosphate (DCP). In addition, it can be used in the production of synthetic detergents and animal feed.
Read MoreOnce the phosphate ore is dried, it can be reacted with sulfuric acid to produce phosphoric acid. Phosphoric acid is a versatile material, used in the creation of many products, but it is most commonly used in the production of phosphatic fertilizers and animal feeds. MCP and DCP are created by reacting the phosphoric acid with calcium ...
Read MoreSingle super phosphate in made by the reaction of phosphate rock with sulphuric acid to connect the insolubic (tribe sic) form of calcium phosphate to a soluble (monobasic) form. This reason can be represented by the following chemical reaction, which is the major reaction. 1. Major reaction. Ca 3 (PO 4) 2 + 2H 2 SO 4 + H 2 O = CaH 4 (PO 4) 2.
Read MorePreparation of monocalcium phosphate slurry is carried out in two stages, at first stage the phosphoric acid is mixed with limestone up to mixture pH =2.9-3.1, at second stage - up to mixture pH =3.5-3.7, during mixing of monocalcium phosphate slurry with lime pH is maintained in the range 5.4-5.6.
Read MoreFollow this APPLICATION TO DICALCIUM PHOSPHATE PROCESS. 43 The manufacturing coats for the normal superphosphate plant are taken from Rounsley (43). dicalcium phosphate production line . Aug 2, 2016 Phosphoric acid is the intermediary product for the manufacturing process of dicalcium phosphate machinery Dicalcium Phosphate, World News .
Read MoreAn investigation was undertaken to develop a process for producing di-calcium phosphate by direct acidulation of phosphate rock. In general, when phosphate rock is treated with sulfuric acid, mono-calcium phosphate or phosphoric acid is formed. If less sulfuric acid is used, di-calcium phosphate should be formed
Read MoreA process is provided for the production of dicalcium phosphate form a phosphate source material in which a solution of phosphoric acid is produced by the action of a suitable mineral acid, generally sulphuric acid, on a phosphate source material.
Read MoreThe process of the present study was the traditional wet-process for phosphoric acid manufacture. This is one of the most complex processes ... dicalcium phosphate have almost identical crystal structures and under poor control, may form a solid solution resulting in a phosphate loss.
Read MoreThe most common production process used for obtaining dicalcium phosphate dihydrate is dissolving either rock phosphate or bones in hydrochloric acid, purification and precipitation in crystals. Under very precise and controlled process parameters dicalcium phosphate dihydrate can also be produced from purified feed grade phosphoric acid with
Read MoreUS2948590A Process for the manufacture of dicalcium . US2948590A US636468A US63646857A US2948590A US 2948590 A US2948590 A US 2948590A US 636468 A US636468 A US 636468A US 63646857 A US63646857 A US 63646857A US 2948590 A US2948590 A US 2948590A Authority US United States Prior art keywords acid phosphoric acid slurry dicalcium phosphate weight Prior art
Read MoreThe most common method, however, is to defluorinate phosphoric acid and react it with lime to get dicalcium phosphate. Sulfuric Acid: This acid is produced at phosphate plants for use in reacting with phosphate rock to produce phosphoric acid. The heat generated off sulfuric acid production is used to power phosphate manufacturing plants and ...
Read MoreThe process for fertilizer manufacture based on the transformation of sulfur to sulfuric acid, reacts it with phosphate rock, then rejects it as gypsum contaminated with radium.
Read MoreDicalcium phosphate is used as a food additive, it is found in some toothpastes as a polishing agent and is a biomaterial. Manufacturing Process. 1. Dibasic calcium phosphate is produced by the neutralization of calcium hydroxide with phosphoric acid, which precipitates the dihydrate as a solid. At 60 °C the anhydrous form is precipitated:
Read MoreDec 01, 2003 The rock phosphate is first digested with sulphuric acid, yielding phosphoric acid. After further filtration, purification and defluorination steps, this “feed grade” phosphoric acid is reacted with a calcium source such as quicklime and/or limestone under strictly controlled conditions. Thus, anhydrous dicalcium phosphate (CaHPO4) is formed.
Read MoreSingle super phosphate in made by the reaction of phosphate rock with sulphuric acid to connect the insolubic (tribe sic) form of calcium phosphate to a soluble (monobasic) form. This reason can be represented by the following chemical reaction, which is the major reaction. 1. Major reaction. Ca 3 (PO 4) 2 + 2H 2 SO 4 + H 2 O = CaH 4 (PO 4) 2.
Read MoreDicalcium phosphate is the calcium phosphate with the formula CaHPO 4 and its dihydrate. The "di" prefix in the common name arises because the formation of the HPO 4 2– anion involves the removal of two protons from phosphoric acid, H 3 PO 4.It is also known as dibasic calcium phosphate or calcium monohydrogen phosphate.Dicalcium phosphate is used as a food additive, it is found in some ...
Read MoreRock Based Dicalcium Phosphate. As a Rock Phosphate Wholesale Manufacturer, we feel that the production process makes a big difference. The most common form of manufacturing is called the ‘wet acid’ method. In this method, the rock phosphate is made to react with concentrated Sulphuric Acid. This releases phosphoric acid, which is further ...
Read MoreManufacturing of dicalcium phosphate process are of two types , first is direct phosphoric acid with calcium oxide reaction and second is based on the reaction with sulphuric acid and rock phosphate powder to produce single super phosphate. If we use phosphoric acid for dcp production than first we make phosphoric acid with sulphuric acid 98% ...
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